MEMS压电-磁电复合式振动能量采集器

具有高能量输出密度的自我供电振动能量采集技术有着迫切的应用需求,是智能化MEMS器件系统发展的重要方向。研究了一种可将外界环境振动能转化为电能的MEMS压电-磁电复合振动能量采集器,其综合了压电发电和磁电发电的优势,为新型MEMS供电研究提供了新思路。利用溶胶-凝胶工艺完成锆钛酸铅(PZT)压电功能薄膜的制备,采用MEMS加工技术完成器件四悬臂梁-中心质量块基础结构的设计和制作,结合集成封装技术实现微结构与永磁铁的微组装。测试结果表明:在一阶谐振频率247 Hz,10 g加速度激励的振动状态下,器件压电部分压电敏感单元与磁电部分电感线圈的单位体积最大有效输出电压分别为2.066×107和5.002×106 mV/cm3。     

采用吸气管过热度调节的户式空气源采暖空调热水三用机

简要介绍户式空气源采暖空调热水三用机的项目背景、技术原理、技术路线。针对三用机的特殊技术要求,首次提出吸气管过热度的定义以及采用电子膨胀阀PID调节吸气管过热度的新概念,利用该调节方法研制一台三用机,并按行业标准进行型式试验检测。测试结果表明,三用机达到国标的节能等级,并可高效制热、低温采暖,以及实现高效率的采暖、空调、热水、空调＋热水等功能。     

Magnetic Anomalies and Spin-Glass-Like Behavior in Ce2CuGe6

A Ce-based intermetallic compound Ce₂CuGe₆ and its La analogue La₂CuGe₆ were synthesized and examined by X-ray powder diffraction, electrical resistivity, magnetic susceptibility, X-ray absorption spectrum and specific-heat measurements. The results reveal that Ce₂CuGe₆ is an antiferromagnetic Kondo-lattice compound with T _N ∼15 K. The effective moment deduced from paramagnetic region is 2.58 μ _B per cerium ion, which is close to localized Ce³⁺ free ion in ²F_5/2 state. X-ray absorption measurement also precluded the existence of an intermediate valence state. The magnetic entropy calculated from heat capacity specific-heat measurement suggested a doublet ground state. In addition, we also observed a spin-glass-like behavior in this material. The spin-glass-like behavior might be due to the complex interplay between magnetic interactions.     

Nanodevices: Location of Biomarkers and Reagents within Agarose Beads of a Programmable Nano‐bio‐chip (Small 5/2011)

The slow development of cost‐effective medical microdevices with strong analytical performance characteristics is due to a lack of selective and efficient analyte capture and signaling. The recently developed programmable nano‐bio‐chip (PNBC) is a flexible detection device with analytical behavior rivaling established macroscopic methods. The PNBC system employs ≈300 μm‐diameter bead sensors composed of agarose “nanonets” that populate a microelectromechanical support structure with integrated microfluidic elements. The beads are an efficient and selective protein‐capture medium suitable for the analysis of complex fluid samples. Microscopy and computational studies probe the 3D interior of the beads. The relative contributions that the capture and detection of moieties, analyte size, and bead porosity make to signal distribution and intensity are reported. Agarose pore sizes ranging from 45 to 620 nm are examined and those near 140 nm provide optimal transport characteristics for rapid (<15 min) tests. The system exhibits efficient (99.5%) detection of bead‐bound analyte along with low (≈2%) nonspecific immobilization of the detection probe for carcinoembryonic antigen assay. Furthermore, the role analyte dimensions play in signal distribution is explored, and enhanced methods for assay building that consider the unique features of biomarker size are offered.     

Relation Between Viscosity and Electrical Conductivity of Silicate Melts

The relation between viscosity and electrical conductivity of binary silicate melts is studied. The logarithm of viscosity varied linearly with the logarithm of conductivity. Furthermore, the lines are different for a MO-SiO₂ system than for a M₂O-SiO₂ system. Compared with the MO-SiO₂ system, the viscosity of the M₂O-SiO₂ system decreases more with the increase in conductivity.     

Secure Software Configuration Management Processes for nuclear safety software development environment

The main difference between nuclear and generic software is that the risk factor is infinitely greater in nuclear software – if there is a malfunction in the safety system, it can result in significant economic loss, physical damage or threat to human life. However, secure software development environment have often been ignored in the nuclear industry. In response to the terrorist attacks on September 11, 2001, the US Nuclear Regulatory Commission (USNRC) revised the Regulatory Guide (RG 1.152-2006) “Criteria for use of computers in safety systems of nuclear power plants” to provide specific security guidance throughout the software development life cycle. Software Configuration Management (SCM) is an essential discipline in the software development environment. SCM involves identifying configuration items, controlling changes to those items, and maintaining integrity and traceability of them. For securing the nuclear safety software, this paper proposes a Secure SCM Processes (S²CMP) which infuses regulatory security requirements into proposed SCM processes. Furthermore, a Process Flow Diagram (PFD) is adopted to describe S²CMP, which is intended to enhance the communication between regulators and developers.     

丁烯氧化脱氢铁系催化剂绿色制备关键因素的考察

丁烯氧化脱氢是工业生产丁二烯常用的工艺,其中,铁系催化剂是丁烯氧化脱氢工业使用的主流催化剂,为满足清洁生产的需要,了解催化剂制备过程中产生的NOx及废水等排放物的组成尤为重要。对铁系催化剂生产过程中前驱体制备步骤的气体生成及组成进行研究,同时对沉淀洗涤步骤产生的废液成分进行检测。通过XRD、TG-DSC、ICP和TPC等技术对催化剂性质及制备排放物进行分析,考察制备条件对催化剂结构和性能的影响及废物排放的变化规律。结果表明,在前驱体制备溶铁过程中,空气气氛下提高硝酸浓度可有效抑制氢气的产生;不同焙烧温度阶段,生成NOx种类有较大差别;排放废水中含有较多的Zn离子。焙烧条件试验表明,最佳焙烧温度为(650~700)℃,焙烧时间低于9 h。     

Bioactive Chemical Constituents from the Brown Alga Homoeostrichus formosana

A new chromene derivative, 2-(4'',8''-dimethylnona-3''E,7''-dienyl)-8-hydroxy-2,6-dimethyl-2H-chromene (1) together with four known natural products, methylfarnesylquinone (2), isololiolide (3), pheophytin a (4), and β-carotene (5) were isolated from the brown alga Homoeostrichus formosana. The structure of 1 was determined by extensive 1D and 2D spectroscopic analyses. Acetylation of 1 yielded the monoacetylated derivative 2-(4'',8''-dimethylnona-3''E,7''-dienyl)-8-acetyl-2,6-dimethyl-2H-chromene (6). Compounds 1–6 exhibited various levels of cytotoxic, antibacterial, and anti-inflammatory activities. Compound 2 was found to display potent in vitro anti-inflammatory activity by inhibiting the generation of superoxide anion (IC₅₀ 0.22 ± 0.03 μg/mL) and elastase release (IC₅₀ 0.48 ± 0.11 μg/mL) in FMLP/CB-induced human neutrophils.     

Sinterability of Forsterite Prepared via Solid‐State Reaction

In this work, the sinterability of forsterite powder synthesized via solid‐state reaction was investigated. X‐ray diffraction (XRD) analyses indicate that the synthesized powder possessed peaks that correspond to stoichiometric forsterite. Scanning electron micrographs revealed that the powders were formed agglomerates, which were made up of loosely packed fine particles. Subsequently, the forsterite powders were cold isostatically pressed into a disk shape under 200 MPa and sintered in air at temperature ranging from 1200°C to 1500°C (interval of 50°C) with ramp rate of 10°C/min and dwelling time of 2 h. The sinterability of each sintered samples was examined in terms of phase stability, relative density, Vickers hardness, fracture toughness, and microstructural examination. XRD examination on all the sintered samples exhibited pure forsterite, in which the generated peaks were found to be in a good agreement with JCPDS card no. 34‐0189. The densification of forsterite progressed to reach a maximum relative density of ~91% at 1500°C. This study also revealed that high‐strength forsterite ceramic can be synthesized via solid‐state reaction as forsterite attained favorable mechanical properties, having fracture toughness of 4.88 MPam^1/2 and hardness of 7.11 GPa at 1400°C.